(Ebook PDF) Handbook on Miniaturization in Analytical Chemistry Application of Nanotechnology 1st Edition by Chaudhery Mustansar Hussain 012822553X 9780128225530 full chapters

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ISBN-10 :  012822553X 

ISBN-13 :  9780128225530

Author : Chaudhery Mustansar Hussain 

Handbook on Miniaturization in Analytical Chemistry: Application of Nanotechnology provides a source of authoritative fundamentals, interdisciplinary knowledge and primary literature for researchers who want to fully understand how nano-technologies work. Covering all stages of analysis, from sample preparation to separation and detection, the book discusses the design and manufacturing technology of miniaturization and includes an entire section on safety risks, ethical, legal and social issues (ELSI), the economics of nanotechnologies, and a discussion on sustainability with respect to nano- and lab-on-chip technologies.

Handbook on Miniaturization in Analytical Chemistry: Application of Nanotechnology 1st Table of contents:

Chapter 1 Era of nano-lab-on-a-chip (LOC) technology
1 Introduction
2 Lab-on-a-chip technology
2.1 Paper-based LOC systems
2.2 Centrifugal LOC systems
2.3 Droplet-based LOC systems
2.4 Digital LOC systems
2.5 Surface acoustic wave-based LOC systems
3 Applications of LOC technology
3.1 LOC platforms for biological applications
3.2 LOC platforms for environmental applications
3.3 LOC platforms for food applications
4 Conclusions
References
Section A Sample preparation stage of analysis
Chapter 2 Microfluidics in lipid extraction
1 Introduction to biodiesel production from lipids
2 Positive attributes of microfluidics over existing technologies
3 Ideal characteristics of microfluidic devices
4 Design of microfluidic devices in lipid extractions from microalgae/oleaginous microbes
4.1 Reservoir with filter design
4.2 Lab-on-a-disc design
4.3 Bead-packed microchannel design for lipid extraction
4.4 U-shaped trap split-channel design
4.5 Confined impinging jet mixer design
5 Lipid extractions from microalgae and oleaginous microorganisms
6 Future prospects
7 Conclusion
Websites
References
Chapter 3 Microfluidic strategies for extraction and preconcentration of proteins and peptides
1 Introduction
2 Electrokinetic preconcentration
2.1 Field-amplified sample injection
2.2 Isotachophoresis
2.2.1 ITP-based isolation
2.2.2 ITP-based immunoassays
2.2.3 ITP in microchip gel electrophoresis
2.3 Isoelectric focusing
2.4 Multidimensional analysis
3 Preconcentration on solid supports
3.1 Methodology based on molecular recognition mechanism
3.2 Monoliths
3.2.1 General features
3.2.2 Applications
3.3 Beads
3.4 Membranes
3.5 Emerging microfluidic strategies for protein preconcentration
4 Conclusion and futures perspectives
References
Chapter 4 The role of magnetic nanomaterials in miniaturized sample preparation techniques
1 Introduction
2 Magnetic nanomaterial synthesis
2.1 Coprecipitation
2.2 Hydrothermal synthesis
2.3 Microemulsion
2.4 Thermal decomposition
2.5 Sonochemical
3 Surface functionalization of magnetic nanomaterials: Coatings
3.1 Silica
3.2 Surfactants
3.3 Ionic liquids
3.4 Polymers
3.5 Molecularly imprinted polymers
3.6 Carbon and derivatives
4 Application of magnetic nanomaterials in sample preparation
5 Conclusion
References
Further reading
Chapter 5 Miniaturized methods of sample preparation
1 Introduction
2 Solid-phase microextraction techniques
2.1 On-fiber SPME
2.2 Solid-phase dynamic extraction
2.3 Matrix solid-phase dispersion
2.4 Sea sand disruption method
2.5 Stir bar sorptive extraction
2.6 Microextraction in packed syringe
2.7 QuEChERS
3 Liquid-phase microextraction techniques
3.1 Single-drop microextraction
3.2 Hollow-fiber liquid phase microextraction
3.3 Electromembrane extraction
3.4 Dispersive liquid-liquid microextraction
3.5 Supported liquid extraction
3.6 Cloud point extraction
3.7 Salt-assisted liquid-liquid extraction
4 Conclusions
Websites
References
Section B Separation/identification stage of analysis
Chapter 6 Lab-on-chip for chromatographic techniques
1 Introduction
2 Lab-on-chip and chromatography-on-chip
3 Liquid chromatography on-chip
4 Gas chromatography-on-chip
5 Conclusions
References
Chapter 7 Lab on a chip: A versatile integration with spectroscopic techniques
1 Introduction
2 Biomolecular spectroscopy
2.1 Raman spectroscopy and fluorescence spectroscopy
2.2 Surface-enhanced Raman spectroscopy
3 Functionality of lab-on-a-chip devices
4 Applications of LOC-Raman/SERS
5 Applications of fluorescence spectroscopy
Website
References
Section C Detection stage of analysis
Chapter 8 Contactless conductivity detection on lab-on-a-chip devices: A simple, inexpensive, and po
1 Introduction
2 Principle and theory of C4D
2.1 Electronic circuit for C4D detectors
2.2 Cell geometry and electrode design
3 Microsystems and portability
4 Fabrication of sensing electrodes
4.1 Metal electrodes
4.2 Nonmetallic electrodes
5 Applications
5.1 Bioanalytical studies
5.2 Clinical applications
5.3 Environmental applications
5.4 Forensics
5.5 Other applications
6 Conclusions
Acknowledgments
References
Chapter 9 Multidimensional sensors: Classification, nanoprobes, and microfluidics
1 Introduction
2 Classification
2.1 Type A: Heterogeneous probe/sample interactions
2.1.1 Type A1
2.1.2 Type A2
2.1.3 Type A3
2.1.4 Type A4
2.2 Type B: Multichannel outputs
2.2.1 Type B1
2.2.2 Type B2
2.3 Type C: Heterogeneous probe/sample interactions and multichannel outputs
3 Nanomaterials for high-performance multidimensional sensors
3.1 Improving the sensitivity and recognition ability
3.2 Lab-on-a-nanomaterial
3.3 Single probe and measurement
4 Microfluidic platforms
5 Conclusion and outlook
Websites
Acknowledgments
References
Chapter 10 Miniaturized microfluidic heuristics for the detection of polluting molecules in the envi
1 Introduction: Environmental pollutants
1.1 Heavy metals
1.2 Pesticides
1.3 Organophosphorus compounds
1.4 Xenobiotics
2 Existing detection strategies for environment pollutants and their drawbacks
2.1 Detection of heavy metals
2.2 Detection of xenobiotics
2.3 Detection of pesticides
3 Positive attributes of microfluidics for better detection of environmental pollutants
4 Designs for detection
4.1 Colorimetric approach
4.2 Electrochemical approach
4.3 Other optical methods
5 Future scope
6 Conclusion
References
Section D Important aspects and challenges
Chapter 11 Pushing the limits of analytical characterization tools: How much is too much?
1 Introduction
2 Theories involving crystallite and grain size measurements
2.1 Issues related to the measurements and analyses of crystallite and grain sizes
2.2 Can X-ray diffraction become “a limiting tool” for phase analyses?
2.2.1 Issues examining phase change via XRD: The fluorite-pyrochlore transition
3 Fundamentals of differential scanning calorimetry
3.1 Measurement issues with the order of phase transition using DSC and/or DTA
3.2 Measurement and interpretation issues with glass transition
3.3 Probing crystallization and associated phase transition events using DSC and/or DTA
4 Conclusion
References
Chapter 12 Future of the modern age of analytical chemistry: Nanominiaturization
1 Introduction
2 Categorization of miniaturized systems
3 Miniaturization of separation techniques
3.1 Miniaturization of liquid chromatography systems
3.2 Miniaturization of gas chromatography systems
3.3 Miniaturization of capillary electrophoresis systems
4 Miniaturization of detection techniques
4.1 Atomic and molecular spectrometry-based detection systems
4.2 Mass spectrometry-based detection systems
4.3 Electrochemical detection systems
5 Conclusions
References
Chapter 13 Nanobiotechnology approaches for miniaturized diagnostics
1 Introduction
2 Nanobiotechnology
3 Nanobiosensors
3.1 Types of nanomaterial
3.1.1 Gold nanoparticles
3.1.2 Silver nanoparticles
3.1.3 Quantum dots
3.1.4 Magnetic nanoparticles
3.1.5 Carbon nanoparticles
3.2 Type of biomaterial
3.2.1 Proteins
3.2.2 Nucleic acids
3.2.3 Aptamers
4 Techniques for the conjugation of biomaterials with nanomaterials
5 Nanobiotechnology-based diagnostic devices
5.1 Principle and mechanism of signal detection in nanobiotechnology-based diagnostic devices
5.2 Commercialized nanobiotechnology-based miniaturized diagnostic devices
6 Advantages and disadvantages of nanobiotechnology-based diagnosis
Acknowledgment
Conflict of interests

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