(EBook PDF) Nanomaterials Synthesis Design Fabrication and Applications 1st edition by Yasir Beeran Pottathara, Sabu Thomas, Nandakumar Kalarikkal, Yves Grohens, Vanja Kokol 0128157526 9780128157527 full chapters

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ISBN-10:   0128157526 

ISBN-13 :  9780128157527

Author :  Yasir Beeran Pottathara, Sabu Thomas, Nandakumar Kalarikkal, Yves Grohens, Vanja Kokol

Nanomaterials Synthesis: Design, Fabrication and Applications combines the present and emerging trends of synthesis routes of nanomaterials with the incorporation of various technologies. The book covers the new trends and challenges in the synthesis and surface engineering of a wide range of nanomaterials, including emerging technologies used for their synthesis. Significant properties, safety and sustainability and environmental impacts of the synthesis routes are explored. This book is an important information source that will help materials scientists and engineers who want to learn more about how different classes of nanomaterials are designed.

Nanomaterials Synthesis: Design, Fabrication and Applications 1st Table of contents:

1 Synthesis and Processing of Emerging Two-Dimensional Nanomaterials
1.1 Introduction
1.2 Emerging 2D Nanomaterials: Uniqueness and Advances
1.3 Synthesis Approaches
1.3.1 Top-Down Approaches
1.3.1.1 Mechanical Cleavage
1.3.1.2 Liquid Exfoliation by Mechanical Force
1.3.1.3 Liquid Exfoliation by Chemical and Electrochemical Ion Intercalation
1.3.1.4 Liquid Exfoliation by Ion Exchange
1.3.1.5 Liquid Exfoliation by Oxidation and Reduction
1.3.1.6 Liquid Exfoliation by Selective Etching
1.3.2 Bottom-Up Approaches
1.3.2.1 Chemical Vapor Deposition
1.3.2.2 Wet-Chemical Synthesis
1.4 Summary and Outlook
References
2 Nanomaterial Synthesis: Chemical and Biological Route and Applications
2.1 Introduction and Background: Nanoparticle Synthesis Approaches
2.2 Different Chemical Routes for Nanomaterial Synthesis
2.2.1 Ultrasound-Assisted Synthesis
2.2.2 Colloid Nanoparticle Synthesis
2.2.3 Nanoparticle Synthesis Using Microreactors
2.3 Nanoparticle Synthesis Using the Biological Route
2.3.1 Plant Extract-Based Nanoparticle Synthesis
2.3.2 Microbial Synthesis of Nanoparticles
2.4 Application of Nanomaterials
2.4.1 Nanoclay and Polymer Nanocomposite and Polymer Functional Nanolatex
2.4.2 Photocatalyst for Degradation of Organic Pollutants
2.5 Recent Advances in the Chemical and Biological Synthesis Routes
2.6 Scale-Up Issues of Nanoparticle Production and Challenges
2.7 Summary
Acknowledgment
References
3 Chemical Approaches for 1D Oxide Nanostructures
3.1 Introduction
3.2 1D Nanostructure Synthesis Techniques
3.3 1D ZnO Nanostructures
3.3.1 Crystal Structure of ZnO
3.3.2 Zinc Oxide Nanostructures: Synthesis Methods
3.3.3 ZnO Nanostructures Through Hydrothermal Growth
3.3.4 Effects of the Hydrothermal Temperature, Growth Solution Concentration, Reaction Strength, and
3.3.5 Doping of ZnO nanostructures Through Hydrothermal Routes
3.3.6 Recent Challenges in Nanotechnology Based on 1D ZnO Nanostructures
3.4 1D TiO2 Nanostructure
3.4.1 Crystal Structure of TiO2
3.4.2 1D TiO2 Nanostructure Synthesis Techniques From Chemical Solution
3.4.2.1 Hydrothermal/Solvothermal Method
3.4.2.2 Sol–Gel Method
3.4.2.3 Surfactant-Assisted Method
3.4.2.4 Microwave-Assisted Method
3.4.2.5 Sonochemical Method
3.4.2.6 Electrospinning Method
3.4.2.7 High-Temperature Pyrolysis Method
3.4.3 Growth Mechanism of 1D TiO2 Nanostructures From Chemical Solution
3.4.3.1 Surfactant-Controlled Growth
3.4.3.2 Oriented Attachment (Surfactant-Free)
3.4.3.3 Dissolve and Grow Mechanism
3.4.4 Recent Synthesis Trends and Challenges in Nanotechnology Based on 1D Nanostructures
3.5 Conclusion
References
4 One- and Two-Dimensional Nanostructures Prepared by Combustion Synthesis
4.1 Introduction
4.2 CS Fundamentals
4.2.1 Thermodynamics
4.2.2 Kinetics
4.3 Microstructural Characteristics of Combustion-Derived Nanomaterials
4.3.1 Solid–Gas and Solid–Solid CS Systems
4.3.1.1 1D Nanostructures
4.3.1.2 2D Nanostructures
4.3.2 Solution Combustion Synthesis
4.3.2.1 1D Nanostructures
4.3.2.2 2D Nanostructures
4.4 Conclusions
References
5 Microwave-Assisted Synthesis for Carbon Nanomaterials
5.1 Introduction
5.2 Methods of Synthesis of Carbon Nanomaterials
5.2.1 Arc Discharge Method
5.2.2 Laser Ablation
5.3 Chemical Vapor Deposition
5.3.1 Chemical Vapor Deposition Substrate Catalyst Method
5.3.2 Metal Catalyst Influence in the Chemical Vapor Deposition Technique
5.4 Plasma-Enhanced Chemical Vapor Deposition-Based Carbon Nanomaterials
5.5 Microwave-Enhanced Chemical Vapor Deposition
5.6 Fluidized Bed Chemical Vapor Deposition
5.7 Vapor Phase Growth Chemical Vapor Deposition
5.8 Microwave-Assisted Synthesis of Graphene
5.9 Future Prospects for Carbon Nanomaterial Synthesis and Challenges
5.10 Conclusion
References
6 Strategies in Laser-Induced Synthesis of Nanomaterials
6.1 Introduction
6.1.1 Long- and Short-Pulse Interaction
6.1.2 Femtosecond Laser–Solid Interactions: Fundamental Processes
6.1.3 Structural Changes Induced by Ultrashort Laser Pulses
6.2 Experimental Fabrication
6.2.1 Synthesis Methods
6.2.2 Characterization Methods
6.2.3 Nonlinear Optical Properties (Z-Scan Studies)
6.3 Results and Discussion
6.3.1 Surface Nanostructuring on Graphite
6.3.2 Formation of Graphene Quantum Dots by Laser Irradiation of Graphite in Water
6.3.3 Ge Nanoparticles by Pulsed Laser Ablation of Ge in Different Liquids
6.3.4 Surface Nanostructuring on Au Film-Coated Si Substrates for Surface-Enhanced Raman Scattering
6.3.5 Blue Luminescent Si Nanoparticle Synthesis by Laser Ablation of Si in Water
6.3.6 Nanostructuring of Titanium Metal Towards Fabrication of Low-Reflective Surfaces
6.3.7 Formation of Metal Nanostructures in a Polymer Matrix by Using Femtosecond Laser Irradiation
6.3.8 Aluminum Nanoparticles Prepared by Laser Ablation in Different Liquids for Application as a Po
6.3.9 Metal Nanoparticles in Liquids (Mo, Ti, In, Au–Ag Alloy, and Al)
6.4 Conclusions
References
7 Flame Synthesis of Nanostructured Transition Metal Oxides: Trends, Developments, and Recent Advanc
7.1 Introduction
7.1.1 Motivation
7.2 Properties and Applications of 1D and 3D Transition Metal Oxide Nanostructures
7.2.1 Solar Panels
7.2.2 Electrochromic Devices
7.2.3 Lithium-Ion Batteries
7.2.4 Capacitors
7.2.5 Gas Sensors
7.2.5.1 Chemical Composition
7.2.5.2 Physical Morphological Properties
7.2.6 Light-Emitting Diodes
7.2.7 Catalysis
7.3 Fabrication Techniques to Synthesize TMO Nanostructures
7.3.1 Chemical Vapor Deposition
7.3.2 Sol–Gel
7.3.3 Plasma
7.3.4 Flames
7.4 Flames as a Unique Fabrication Tool to Produce TMO Nanoparticles
7.4.1 Flame Synthesis of Metal-Oxide Nanoparticles
7.4.2 The “Aerosol” and “Spray Pyrolysis” Methods
7.4.3 Approaches Used for Control Synthesis in “Aerosol” and “FSP”
7.5 Flame Synthesis of Multidimensional TMOs Using the “Solid Support” Method
7.5.1 Parameters Affecting the Flame Synthesis of Multidimensional TMOs
7.5.2 Effect of Probe Diameter and Oxygen Content in the Oxidizer
7.5.3 Effect of Thermal Property of the Source Material—Iron Oxide Structures
7.5.4 Effect of Flame Positon
7.5.5 Hybrid Approach to Form Core–Shell TMOs Through “Solid Support” and Electrodeposition
7.6 Volumetric Flame Synthesis of 1D and 3D TMOs
7.6.1 TMOs (1D) Formed Using “Aerosol” and “Spray Pyrolysis”
7.6.2 “Gas Phase” Flame Synthesis of 1D and 3D TMOs
7.7 Core–Shell and Mixed Transition Metal Oxide Nanostructures
7.7.1 Flame Synthesis of Core–Shell and MTMOs on Solid Substrates
7.7.2 Synthesis of MTMOs and Related Core–Shell Nanostructures Using “Flame Spray Pyrolysis”
7.7.3 Gas-Phase Synthesis of 1D and 3D Core–Shell and MTMOs
7.8 Conclusions
Acknowledgments
References
8 Design and Fabrication of Porous Nanostructures and Their Applications
8.1 Introduction
8.2 Classification of Porous Nanostructures
8.3 Synthesis of Porous Materials
8.3.1 Synthesis of Microporous Materials
8.3.2 Synthesis of Mesoporous Materials
8.3.2.1 Role of Template in the Formation of Porosity
8.3.2.2 Role of Surfactants as Structure-Directing Agents
8.3.3 Synthesis of Macroporous Materials
8.3.4 Synthesis of Purely Organic Porous Materials
8.3.5 Synthesis of Inorganic Nanoporous Materials
8.3.5.1 Silica-Based Mesoporous Materials
8.3.5.2 Nonsilica-Based Mesoporous Materials
8.3.6 Synthesis of Organic–Inorganic Hybrid Polymeric Material
8.4 New Synthesis Approaches and Challenges of Porous Nanostructures
8.5 Applications of Porous Materials
8.5.1 Biomedical Use
8.5.2 Catalysis
8.5.3 Sensors and Supercapacitors
8.5.4 Adsorption, Separation, and Catalytic Conversion of CO2
8.5.5 Food Industry
8.5.6 Water Treatment
8.5.7 Gas Separation, Purification, and Storage
8.5.8 Photocatalyst
8.5.9 Agriculture
8.6 Conclusion
References
9 Synthesis and Processing of Thermoelectric Nanomaterials, Nanocomposites, and Devices
9.1 Introduction to Energy Needs and Wasted Thermal Energy
9.2 Fundamentals of the Thermoelectric Effect and Thermoelectric Materials
9.3 Inorganic Thermoelectric Nanomaterials
9.3.1 Metal Chalcogenides
9.3.1.1 Lead Chalcogenides
9.3.1.2 Bismuth Chalcogenides
9.3.2 Metal Oxides
9.3.3 Superionic Conductors
9.3.4 Silicon-Based Materials
9.3.5 Skutterudites, Clathrates, and Half-Heusler Alloys
9.4 Organic Thermoelectrics: Polymer and Nanocomposite Systems
9.4.1 Conjugated Polymer Thermoelectric Materials
9.4.2 Nanocomposite Polymer Thermoelectric Materials
9.5 Working Principle and Specific Architectures of Thermoelectric Generators
9.6 Application of Thermoelectric Generators
9.7 Recent Trends and Challenges
9.7.1 Market for Thermoelectric Generators and Recent Technologies in Thermoelectric Materials and D
9.7.2 Challenges in Potential Thermoelectric Generator Applications
9.8 Future Perspectives
9.9 Summary and Conclusions
Acknowledgment
References
10 Fabrication Techniques of Group 15 Ternary Chalcohalide Nanomaterials
10.1 Introduction
10.2 Fabrication of Composite Materials
10.2.1 Nanocomposites of SbSI Dots in Sodium Borosilicate Glass
10.2.2 Nanocomposites of SbSI Dots in Organically Modified Titanium Dioxide Glass
10.2.3 Electrospinning of Fibers and Mats
10.2.4 Fabrication of Piezoelectric Paper
10.3 Ball Milling of Bulk Crystals
10.4 Vapor-Phase Growth of SbSI Nanorods
10.5 Graphoepitaxy
10.6 Sonochemical Synthesis of SbSI-Type Nanowires
10.7 Ultrasonic Spray Pyrolysis
10.8 Filling of Carbon Nanotubes
10.9 Solution Processing
10.10 Microwave-Assisted Aqueous Synthesis
10.11 Hydrothermal Growth
10.12 Conversion of Sb2S3 Into SbSI
10.12.1 Conversion by Physical Vapor Method
10.12.2 Conversion by Spinning Coating SbI3 Solution
10.13 Heat and Laser Formation of SbSI Nano-Objects in Chalcohalide Glasses
10.13.1 Growth Activated by Heat Treatment
10.13.2 Laser-Induced Growth
10.14 New Trends in Fabrication Techniques
10.15 Future Perspectives
10.16 Summary
References
11 Advanced Carbon Materials for Electrochemical Energy Storage
11.1 Introduction
11.2 Carbon Materials: Types and Sources
11.2.1 Graphene
11.2.2 Fullerene
11.2.3 Carbon Nanotubes
11.2.4 Biomass-Derived Carbon Materials
11.2.5 Heteroatom-Doped Carbon Materials
11.3 Carbon Materials for Energy Storage
11.3.1 Lithium-Ion Batteries
11.3.2 Sodium-Ion Batteries
11.3.2.1 Carbon-Based Electrode Materials for NIBs
11.3.2.2 Carbon-Based Composite Electrode Materials for NIBs
11.3.3 Other Battery Systems
11.3.4 Supercapacitors
11.4 Challenges and Future Perspectives
Acknowledgments
References
12 Organic–Inorganic Hybrid Nanomaterials: Synthesis, Characterization, and Application
12.1 Introduction
12.2 Interfacial Charge Transfer Complexes: Formation Mechanism and Optical Properties
12.3 Polymer Supports Decorated With Inorganic Nanoparticles
12.4 New Synthetic Approaches and Challenges
12.5 Potential Application of Organic–Inorganic Hybrids: Photo-Driven Processes and Antimicrobial
12.6 Summary and Outlook
Acknowledgments
References
13 Fabrication, Characterization, and Optimization of MnxOy Nanofibers for Improved Supercapacitive
13.1 Introduction
13.2 Synthesis of 1D Nanofibers
13.2.1 Drawing Method
13.2.2 Template Method
13.2.3 Phase Separation
13.2.4 Self-Assembly
13.2.5 Electrospinning
13.2.5.1 Setup and Working Principle
13.2.5.2 Effects of System/Process Parameters on the Nanofibric Morphology
13.2.5.2.1 Effect of Applied Voltage
13.2.5.2.2 Effect of Solution Flow Rate
13.2.5.2.3 Effect of Needle Diameter
13.2.5.2.4 Effect of Distance Between Needle and Collector
13.2.5.2.5 Effect of Polymer Concentration
13.2.5.2.6 Effect of the Molecular Weight of Polymer Used
13.2.5.2.7 Effect of Surface Tension
13.2.5.2.8 Effect of Conductivity/Surface Charge Density
13.2.5.2.9 Effect of Surrounding Temperature and Humidity
13.3 Utilization of Binary MnxOy Nanofibers for Energy-Storage Applications
13.4 Future Aspects, Challenges, and Summary
Acknowledgments
References
14 Fabrication of Micro/Nano-Miniaturized Platforms for Nanotheranostics and Regenerative Medicine A
14.1 Nanotheranostics and Regenerative Medicine: Introduction
14.1.1 Regenerative Medicine and Tissue Engineering
14.1.2 Organ-Specific Bioengineering
14.2 Bioartificial Organs: Introduction
14.2.1 Types of Bioartificial Organs
14.2.2 Scope of Research Into Bioartificial Organs
14.2.3 Bioartificial Organs and Theragnostics
14.3 Micro- and Nanofluidic Devices: Introduction
14.3.1 Micro- and Nanofluidic Cell Culture Devices
14.3.2 Micro- and Nanofluidic Drug-Screening Devices
14.3.3 Micro- and Nanofluidic Biosensing Devices
14.4 Biomimetics: Introduction
14.4.1 Nanostructured Biomimetics
14.4.2 Scaffolding for Biomimetics
14.5 Biopatterning the Complexities of Life: Introduction
14.5.1 Biopatterning the Microstructures
14.5.2 Biopatterning the Nanostructures
14.5.3 Fluidic Simulations on Patterned Surfaces
14.5.4 Bioreactors for In Situ Simulations
14.5.5 Complexities in Biopatterning
14.6 Bioprinting of Organs and Tissues
14.6.1 History of Bioprinting
14.6.2 Techniques Used in Bioprinting
14.6.2.1 Extrusion Bioprinting
14.6.2.2 Laser-Assisted Bioprinting
14.6.2.3 Inkjet Bioprinting
14.6.3 Applications of Bioprinting
14.6.4 Organ Specific Bioprinting
14.6.5 Complexities in Bioprinting
14.7 Conclusions
References
15 Recent Trends in the Synthesis of Carbon Nanomaterials
15.1 Fullerenes
15.1.1 Pristine Fullerenes
15.1.2 Endohedral Fullerenes From Carbon Sources
15.1.3 Endohedral Fullerenes From Pristine Fullerenes
15.1.4 Exohedral Fullerenes
15.1.4.1 Carbene Addition
15.1.4.2 Bingel–Hirsch Reaction
15.1.4.3 Prato Reaction
15.1.4.4 Other Reactions Used
15.2 Carbon Nanotubes
15.2.1 Carbon Nanotube Synthesis and Production
15.2.2 Functionalization of Carbon Nanotubes
15.2.3 Biobased Synthetic Routes
15.3 Graphene
15.3.1 Graphene Synthesis and Production
15.3.1.1 Micromechanical Cleavage
15.3.1.2 Liquid-Phase Exfoliation
15.3.1.3 The Graphite Oxide Route
15.3.1.4 Electrochemical Exfoliation
15.3.1.5 Chemical Vapor Deposition
15.3.1.6 Epitaxial Growth of Graphene on Silicon Carbide Substrate
15.3.2 Biobased Synthetic Routes
15.3.3 Chemical Synthesis
15.3.4 Graphene Heterostructures
15.3.5 Graphene Nanocomposites
15.3.6 Heteroatom-Doped Graphene
15.3.7 Halogenated Graphenes
15.3.8 Hydrogenated Graphenes
15.3.9 Chemical Functionalization of Graphene
15.4 Graphene Nanoribbons
15.5 Carbon Dots
15.5.1 Carbon Dot Synthesis
15.5.1.1 Top-Down Methods
15.5.1.2 Bottom-Up Methods
15.5.1.3 Surface Passivation
15.5.1.4 Doping
15.5.2 Biobased Synthesis Routes
15.6 Challenges and Future Perspectives

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Nanomaterials Synthesis,Design,Fabrication,Applications,Yasir Beeran Pottathara,Sabu Thomas,Nandakumar Kalarikkal,Yves Grohens,Vanja Kokol